Fourier Transform Near-Infrared Spectroscopy Used for Purity Determination of Rhein-L-arginine Cocrystal (Argirein)

作者: Chi ZL, Wang MM, Yang L, Li XM, Cong XD, Liu SG, Cai BC
成果类型: 期刊论文
数据来源: ESI SCIE
发表日期: 2013
年卷期页: 2013,29,(6),661-664
期刊名: 《ANALYTICAL SCIENCES》 影响因子和分区 年份    影响因子    区号
2016    1.228        4区 2015    1.174        4区 2014    1.394        4区 2013    1.569        4区 2012    1.391        4区
缩写刊名: ANAL SCI
英文摘要: A method is described using rapid and sensitive Fourier transform near-infrared spectroscopy (FT-NIRS) for the determination of rhein-L-arginine cocrystal (argirein). By mixing different values of argirein into different proportions with rhein and arginine, we obtained 41 batches of samples to determine. Partial least squares (PLS) regression was selected as the analysis type and standard normal variate (SNV) and original spectra were adopted for the spectral pretreatment. The correlation coefficient (R) of the calibration model was above 0.99 and the root mean square error of predictions (RMSEP) was under 0.012. The developed model was applied to 10 batches of known samples with satisfactory results. The established method is validated and can be applied to the intrinsic quality control of synthetic products and other cocrystals.
语言: English
出版类型: Article
主题: Chemistry, Analytical;Chemistry
作者地址: [Chi, Zongliang; Wang, Miaomiao; Li, Xiaomeng; Cong, Xiaodong; Liu, Shaoguang; Cai, Baochang] Zhejiang Chinese Med Univ, Res Ctr TCM Proc Technol, Hangzhou, Zhejiang, Peoples R China
[Yang, Lin] Univ Otago, Sch Pharm, Dunedin, New Zealand
[Cai, Baochang] Nanjing Univ Chinese Med, Ctr Engn, State Minist Educ Standardizat Chinese Med Proc, Nanjing, Jiangsu, Peoples R China
[Cai, Baochang] Nanjing Univ Chinese Med, Natl First Class Key Discipline Tradit Chinese Me, Nanjing, Jiangsu, Peoples R China
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